NMR-Spectroscopy

Responsible Persons:

Prof. Dr. Heiko Möller
Dr. Matthias Heydenreich (phone: 5199)
Angela Krtitschka (phone: 5158)

Equipment:

  • Bruker Avance 300 MHz Spectrometer
  • Bruker Avance 500 MHz Spectrometer
  • Bruker Avance III 600 MHz Spectrometer
Delivery of samples:
open-access-service
Lab: H.25 E0.06-0.08
Office hours: Mo-Thu: 9.00 a.m. - 3.00 p.m.
Fr: 9.00a.m. - 2.00 p.m.
Out of office hours only by telephone agreement!

Instructions for sample preparation

Tubes and caps:
  • Use only absolutely unpolluted tubes and caps!
  • Minimum length of tubes: 17,8 cm (7'')
  • It is not allowed to use breaked tubes
Solvents and filling height:
  • Use only deuterated solvents!
  • Filling height must be between 4 and 5 cm.
Concentration:
  • 1H : minimum 0,01 mol/l
  • 13C: minimum 0,1 mol/l
Labeling of samples:
  • Use the following labels (Word-Document).
  • More instructions you'll find here (german)
Samples which do not satisfy these requirements will be rejected!
All experiments will be run on the Avance 300 NMR spectrometer. Running at another field strength is only possible after an individual agreement.
All users of the open-access-service have to read and understand tzhe safety instructions of the NMR Lab. This will be documented by signature. The saety insructions you'll find here.